Hi ,

Anybody came across this problem ?

Using the same instrument method ::

I set up a sample set using wizard and calibrate at the beginning (bracketing stds)
The headspace picks up vial, moves to oven then instrument failure occurs and HS vial

I removed the calibrate function from the sample set and it carried out vial preparation as normal and acquired data once injected

Any thoughts why it should fail with calibrate/quantitate commands ?