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system suitability

Posted: Mon Mar 10, 2008 11:48 am
by yamani
dear all
can any one tells me about the procedure for system suitability in LC/MS/MS because in our labs we do the following: we run 6 high concentration samples from the same vial and calculate the CV which must be < 6

Posted: Mon Mar 10, 2008 12:01 pm
by JGK
My previous lab, we ran six injections and using data from the final five (in case of a partially primed injector on the first) with a CV criteria of ≤ 5%