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inorganic mass spec
Posted: Thu Jun 19, 2008 8:31 pm
by tilly
Please can anyone give me some pointers on the use of inorganic mass spectrometry. Like what types of analysis, ionisation techniques. I wonder if anyone has read any basic texts on this that could recommend.
I've a little about seciation analysis but am feeling rather lost. Has anyone any experience of these techniques they could share?
Posted: Thu Jun 19, 2008 8:32 pm
by tilly
sorry that should read speciation ...
Posted: Fri Jun 20, 2008 5:56 pm
by JI2002
ICP-MS is usually used for metal analysis. You need to have a HPLC, IC or other chromatographic tools before ICP-MS for speciation analysis.
Posted: Sun Jun 22, 2008 6:55 pm
by msuk
try this text?
Mass spectrometry of inorganic, coordination and organometallic compounds
/ William Henderson & J. Scott McIndoe.
ISBN 0-470-85015-9
Posted: Mon Jun 23, 2008 7:11 pm
by tilly
thanks for replies,
I'll try to order the book from the library and see if i can make sense of it.
Posted: Mon Nov 03, 2008 1:33 pm
by sindhu
ICP-MS is best suited for Inorganic MS analysis. Better you do Ion Chromatography before analysis
Posted: Wed Nov 05, 2008 9:30 am
by Patrik Appelblad
Another viable alternative would be to use HILIC coupled with ICP-MS.
Recently there has been papers published on this new combination of analytical techniques.
Hydrophilic Interaction Liquid Chromatography (HILIC) Coupled to Inductively Coupled Plasma Mass Spectrometry (ICPMS) utilizing a Mobile Phase with a Low-Volatile Organic Modifier for the Determination of Cisplatin, and its Monohydrolyzed Metabolite
Y. Nygren, P. Hemström, C. Åstot, P. Naredi, E. Björn
J. Anal. At. Spectrom., 23 (2008) 948-954
Alternative Organic Solvents for HILIC Separation of Cisplatin Species with On-Line ICP-MS Detection
P. Hemström, Y. Nygren, E. Björn, K. Irgum
J. Sep. Sci., 31 (2008) 599-603